nucВестник НЯЦ РКNNC RK Bulletin1729-75161729-7885Национальный ядерный центр Республики Казахстан10.52676/1729-7885-2023-3-121-128nuc-549Research ArticleСтатьиСИНТЕЗ НАНОПРОВОЛОК ОРТОРОМБИЧЕСКОГО ДИОКСИДА ОЛОВА В ТРЕКОВЫХ ТЕМПЛЭЙТАХSYNTHESIS OF ORTHORHOMBIC TIN DIOXIDE NANOWIRES IN TRACK TEMPLATESДжунисбековаД. А.JunisbekovaD. A.

Диана Алтаевна Джунисбекова – докторант.

Астана

Astana

diana911115@gmail.comДаулетбековаА. К.DauletbekovaA. K.

Алма Кабдиновна Даулетбекова - кандидат физико-математических наук, профессор.

Астана

Astana

alma_dauletbek@mail.ruБаймухановЗ. К.BaimukhanovZ. K.

Зейн Кайрбекович Баймуханов - кандидат физико-математических наук, доцент.

Астана

Astana

zeinb77@mail.ruБаубековаГ. М.BaubekovaG. M.

Гулдар Мусалиевна Баубекова - PhD доктор, и.о. доцента.

Астана

Astana

guldar_87@mail.ruАкылбековаА. Д.AkylbekovaA. D.

Айман Дуйсембаевна Акылбекова - PhD доктор, старший преподаватель.

Астана

Astana

aiman88_88@mail.ruНАО «Евразийский национальный университет им. Л.Н. Гумилева»КазахстанL.N. Gumilyov Eurasian National UniversityKazakhstan20233009202303121128Copyright © Джунисбекова Д.А., Даулетбекова А.К., Баймуханов З.К., Баубекова Г.М., Акылбекова А.Д., 20232023Джунисбекова Д.А., Даулетбекова А.К., Баймуханов З.К., Баубекова Г.М., Акылбекова А.Д.Junisbekova D.A., Dauletbekova A.K., Baimukhanov Z.K., Baubekova G.M., Akylbekova A.D.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://journals.nnc.kz/jour/article/view/549

В данной работе проведен синтез орторомбических нанопроволок (НП) SnO2 методом электрохимического осаждения в подготовленный ионно-трековый темплэйт SiO2/Si-p. Трекообразования в структуре SiO2/Si создавались путем облучения на циклотроне ДЦ-60 быстрыми тяжелыми ионами Xe с энергией 200 МэВ (Ф = 108 см−2). Для формирования нанопористых шаблонов использовали 4% водный раствор фтористоводородной кислоты (HF). Электрохимическое осаждение (ЭХО) SnO2 в трековый темплэйт осуществляли при комнатной температуре, напряжение на электродах составляла 1,75 В. При процессе ЭХО, был использован электролит со следующим химическим составом: 6 г/л SnCl2 (Sigma-Aldrich) – 25 мл H2O – 2 мл HCl («хч»; 35%; ρ = 1,1740 г/см3). Морфология поверхности образцов, после процесса ЭХО, исследовались на двухлучевом сканирующем микроскопе Zeiss Crossbeam 540. Фазовый состав, кристаллографическая структура наногетероструктур (SnO2/SiO2/Si) с заполнением нанопор диоксидом олова исследовали с помощью рентгеновской дифракции (XRD) на многофункциональном рентгеновском дифрактометре Rigaku SmartLab. Фотолюминесценция измерялась в оптическом диапазоне 320–600 нм с использованием спектрофлуориметра СМ2203 (Solar). Исследование электрических характеристик синтезированных нанопроволок диоксида олова проводилось с использованием патенциостата VersaStat 3 фирмы Ametek.

В результате была получена наногетероструктура SnO2-НП/SiO2/Si с орторомбической кристаллической структурой нанопроволок SnO2. Фотолюминесценция, возбуждаемая светом с длиной волны 240 нм, имеет низкую интенсивность, возникающую в основном за счет таких дефектов, как кислородные вакансии и междоузельное олово или олово поврежденными связями. Измерение ВАХ показало, что полученная таким образом наногетероструктура SnO2-НП/SiO2/Si содержит массивы p-n переходов.

In this work, the synthesis of orthorhombic SnO2 nanowires (NWs) was carried out by electrochemical deposition into prepared SiO2/Si-p ion-track template. Track formations in the SiO2/Si structure were created by irradiation on a DC-60 cyclotron with swift heavy Xe ions with an energy of 200 MeV (Ф = 108 cm−2). A 4% aqueous solution of hydrofluoric acid (HF) was used to form nanoporous templates. Electrochemical deposition (ECD) of SnO2 into the track template was carried out at room temperature, the voltage at the electrodes was 1.75 V. During the ECD process, an electrolyte with the following chemical composition was used: 6 g/l SnCl2 (Sigma-Aldrich) – 25 ml H2O – 2 ml HCl (“reagent grade”; 35%; ρ = 1.1740 g/cm3). The surface morphology of the samples, after the ECD process, was studied on a Zeiss Crossbeam 540 two-beam scanning microscope. The phase composition and crystallographic structure of nanoheterostructures (SnO2-NP/SiO2/Si) with nanopores filled with tin dioxide were studied using X-ray diffraction (XRD) on a multifunctional X-ray diffractometer Rigaku SmartLab. Photoluminescence was measured in the optical range of 320–600 nm using a CM2203 spectrofluorimeter (Solar). The electrical characteristics of the synthesized tin dioxide nanowires were studied using a VersaStat 3 potentiostat from Ametek.

As a result, a SnO2-NWs/SiO2/Si nanoheterostructure with orthorhombic crystal structure of SnO2 nanowires was obtained. Photoluminescence excited by light with a wavelength of 240 nm has a low intensity, arising mainly due to defects such as oxygen vacancies and interstitial tin or tin with damaged bonds. Measurement of the current-voltage characteristic showed that the SnO2-NP/SiO2/Si nanoheterostructure obtained in this way contains arrays of p-n junctions.

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The authors declare that there are no conflicts of interest present.