nucВестник НЯЦ РКNNC RK Bulletin1729-75161729-7885Национальный ядерный центр Республики Казахстан10.52676/1729-7885-2025-1-64-71nuc-772Research ArticleСтатьиОЦЕНКА ВЛИЯНИЯ ПАРАМЕТРОВ МЕХАНОСИНТЕЗА НА МОРФОЛОГИЮ ПОРОШКОВОЙ СМЕСИ НА ОСНОВЕ МАГНИЯEVALUATION OF THE EFFECT OF MECHANOSYNTHESIS PARAMETERS ON THE MORPHOLOGY OF A MAGNESIUM-BASED POWDER COMPOSITIONhttps://orcid.org/0000-0003-4189-6539МухамедоваН. М.MukhamedovaN. M.

Курчатов

Kurchatov

bakayeva@nnc.kzhttps://orcid.org/0009-0009-9616-3982ОспановаЖ. Н.OspanovaZh. N.

Курчатов

Kurchatov

Ospanova@nnc.kzhttps://orcid.org/0009-0000-5740-9331ӨкенО.OkenO.

Курчатов

Kurchatov

oken@nnc.kzhttps://orcid.org/0000-0002-2188-8075МиниязовА. Ж.MiniyazovA. Zh.

Курчатов

Kurchatov

Miniyazov@nnc.kzhttps://orcid.org/0009-0004-9100-7546ШайкиеваК. С.ShaikievaK. S.

Курчатов

Kurchatov

shaikieva@nnc.kzhttps://orcid.org/0009-0008-4694-2200СабыртаеваА. А.SabyrtayevaА. A.

Курчатов

Kurchatov

sabyrtayeva@nnc.kzhttps://orcid.org/0009-0006-7965-7989АхмедиТ. Д.AkhmediT. D.

Курчатов

Kurchatov

akhmedi@nnc.kzФилиал «Институт атомной энергии» РГП НЯЦ РККазахстанBranch “Institute of Atomic Energy” RSE NNC RKKazakhstan202501042025016471Copyright © Мухамедова Н.М., Оспанова Ж.Н., Өкен О., Миниязов А.Ж., Шайкиева К.С., Сабыртаева А.А., Ахмеди Т.Д., 20252025Мухамедова Н.М., Оспанова Ж.Н., Өкен О., Миниязов А.Ж., Шайкиева К.С., Сабыртаева А.А., Ахмеди Т.Д.Mukhamedova N.M., Ospanova Z.N., Oken O., Miniyazov A.Z., Shaikieva K.S., Sabyrtayeva А.A., Akhmedi T.D.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://journals.nnc.kz/jour/article/view/772

В настоящей статье представлен анализ зависимости фазовых и морфологических изменений в порошковом составе системы Mg-Ni-Ce от парметров механосинтеза. В процессе проведения механосинтеза, выявлено, что на изменения структурных характеристик материала, помимо параметров ускорения и продолжительности,  значительное влияние оказывает соотношение порошка и измельчающих шаров. Результаты микроскопического анализа показали, что при соотношении порошка и шаров 1:10 средний размер частиц в синтезированных смесях составляет 13,76 мкм. В то же время, при применении соотношения 1:30 размер частиц уменьшается до 7,59 мкм. Установлено, что основной фазой во всех образцах является магний. Однако при соотношений 1:30 наблюдается формирование гексагональной кристаллической решетки фазы MgNi и образование фазы CeNi. 

This article presents an analysis of the dependence of phase and morphological changes in the powder composition of the Mg-Ni-Ce system on the parameters of mechanical synthesis. During the mechanical synthesis process, it was found that, in addition to acceleration and duration parameters, the ratio of powder to milling balls has a significant influence on changes in the structural characteristics of the material. The results of the microscopic analysis showed that with a powderto-ball ratio of 1:10, the average particle size in the synthesized mixtures is 13.76 µm. At the same time, when applying a ratio of 1:30, the particle size decreases to 7.59 µm. It was established that magnesium is the primary phase in all samples. However, at a ratio of 1:30, the formation of the hexagonal crystal lattice of the MgNi phase and the emergence of the CeNi phase are identified.

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The authors declare that there are no conflicts of interest present.