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THE METHOD OF STABILIZATION OF WATER PRESSURE DURING THE HIGH-TEMPERATURE CORROSION TESTS OF GRAPHITE MATERIALS OF FISSION AND FUSION REACTORS

https://doi.org/10.52676/1729-7885-2018-4-134-138

Abstract

An important technical problem in the study of high-temperature corrosion of graphite materials and SiC-C structures in water vapor in vacuum is to ensure a stable partial pressure (0.001–1.0 Pa) of water vapor in the sample zone. Since the temperature in the sample zone can reach 1400–1700 K, then it is not possible to locate sensors for measuring the vapor pressure there. The paper proposes a method of using metal surfaces of existing or specially introduced elements of a vacuum system (receivers, tanks, pipelines) as a source of water for their controlled heating. Using the computer model of the gas-vacuum environment of the corrosion plant, the ratio of water pressures at the point of sample location and at the point of sampling of the mass analyzer is calculated. The resulting ratio and the analog signal of the mass analyzer (water peak, 18 amu) are used for PID control of the desorption temperature to achieve the required vapor pressure.

About the Authors

Yevgeniy Chikhray
IETP of al-Farabi KazNU
Kazakhstan
Almaty


Vladimir Shestakov
IETP of al-Farabi KazNU
Kazakhstan
Almaty


Saulet Askerbekov
IETP of al-Farabi KazNU
Kazakhstan
Almaty


Inesh Kenzhina
RSE “Institute of Nuclear Physics” under the Ministry of Energy of the RK
Kazakhstan
Almaty


References

1. Chikhray Y. et al. Corrosion test of HTGR graphite with SiC coating //8th International Topical Meeting on High Temperature Reactor Technology, HTR 2016. – American Nuclear Society, 2016.

2. Redhead P. A. Modeling the pump down of a reversibly adsorbed phase. I. Monolayer and submonolayer initial coverage //Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. – 1995. – Vol. 13. – №. 2. – P. 467–475.

3. Dylla H. F., Manos D. M., LaMarche P. H. Correlation of outgassing of stainless steel and aluminum with various surface treatments //Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. – 1993. – Vol. 11. – №. 5. – P. 2623–2636.

4. Hanson A. L. Desiccant (in McGraw Hill Encyclopedia of Science and Technology) // McGraw Hill. 9th ed. – 2002. – P. 1–100.

5. Deitz V. R., Turner N. H. Introduction of water vapor into vacuum systems and the adsorption by the walls //Journal of Vacuum Science and Technology. – 1970. – Vol. 7. – №. 6. – P. 577–580.

6. Redhead P. A. Foundations of vacuum science and technology. – 1998.

7. Reid R. Vacuum science and technology in accelerators //Cockcroft Institute Lectures. – 2010.

8. Thiel P. A., Madey T. E. The interaction of water with solid surfaces: fundamental aspects //Surface Science Reports. – 1987. – Vol. 7. – №. 6-8. – P. 211–385.

9. Dylla H. F. The problem of water in vacuum systems //CERN Accelerator School. – 2006.

10. Saksaganskii G. L. Molecular flow in complex vacuum systems. – Gordon and Breach. – 1988.

11. https://www.comsol.com/comsol-multiphysics.

12. https://en.wikipedia.org/wiki/PID_controller.


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For citations:


Chikhray Ye., Shestakov V., Askerbekov S., Kenzhina I. THE METHOD OF STABILIZATION OF WATER PRESSURE DURING THE HIGH-TEMPERATURE CORROSION TESTS OF GRAPHITE MATERIALS OF FISSION AND FUSION REACTORS. NNC RK Bulletin. 2018;(4):134-138. (In Russ.) https://doi.org/10.52676/1729-7885-2018-4-134-138

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ISSN 1729-7516 (Print)
ISSN 1729-7885 (Online)